Isolation of white wine volatiles using different sample preparation methods
DOI:
https://doi.org/10.5073/vitis.2005.44.187-193Keywords:
white wine, aroma, liquid-liquid extraction, stir bar sorptive extraction, SBSE, solid-phase microextraction, SPMEAbstract
Three sample preparation methods for gas chromatographic analysis of white wine volatiles were tested. In order to find an adequate replacement for common liquidliquid extraction using 1,1,1-trichlorofluoromethan, headspace solid-phase microextraction (HS-SPME) and stir bar sorptive extraction (SBSE) were tested. SPME and SBSE sample preparations are characterized by rapid and easy handling, small sample size and the possibility of automation, but the recovery of aroma compounds is restricted because of the discrimination properties of the polymer phase. Unlike SPME, the results obtained by SBSE are more similar to those of liquid-liquid extraction.
Downloads
Published
Issue
Section
License
The content of VITIS is published under a Creative Commons Attribution 4.0 license. Any user is free to share and adapt (remix, transform, build upon) the content as long as the original publication is attributed (authors, title, year, journal, issue, pages) and any changes to the original are clearly labeled. We do not prohibit or charge a fee for reuse of published content. The use of general descriptive names, trade names, trademarks, and so forth in any publication herein, even if not specifically indicated, does not imply that these names are not protected by the relevant laws and regulations. The submitting author agrees to these terms on behalf of all co-authors when submitting a manuscript. Please be aware that this license cannot be revoked. All authors retain the copyright on their work and are able to enter into separate, additional contractual arrangements.